Solid state recycling of Mg–Gd–Y–Zn–Zr alloy chips by isothermal sintering and equal channel angular pressing
Available online 12 October 2023
Full Length Article
Yanbo Pei, Hongjun Ma, Meng Yuan, Bugang Teng
Abstract
The Mg-7Gd-4Y-2Zn-0.5Zr alloy chips were successfully recycled throughisothermalsintering andequal channel angular pressing(ECAP). The mechanical properties andmicrostructure evolutionof samples during the recycling process were studied in detail. Theeutecticphases in the as-cast alloy transform into long period-stacking ordered (LPSO) phases afterhomogenization, which can improve the plasticity of the material. After isothermal sintering, the density of the sample is lower than that of the homogenized sample, andoxide filmsare formed adjacent to the bonding interface of the metal chips. Hence, the plasticity of the sintered sample is poor. Dense samples are fabricated after ECAP. Although the grains are not refined compared to the sintered sample, the microstructure becomes more uniform due to recrystallization. Fiber interdendritic LPSO phase and kinked 14H-LPSO phase are formed in the alloy due to theshear deformationduring the ECAP process, which improves thestrengthand plasticity of the sample significantly. Furthermore, the basal texture is weakened due to the Bc route of the ECAP process, which can increase theSchmid factorof thebasal slipsystem and improve the elongation of the sample. After 2 ECAP passes, the fully densified recycled billet shows superior mechanical properties with anultimate tensile strengthof 307.1 MPa and elongation of 11.1%.